Processing and visualizing data from electron backscatter diffraction analysis

EBSD data processing involves several steps, including noise reduction, pattern indexing, and the construction of orientation maps. Noise reduction techniques are applied to enhance the quality of the patterns, making them more amenable to accurate indexing. Pattern indexing is performed by matching the experimental patterns to simulated patterns, allowing for the determination of the crystal orientation at each point on the sample surface. The indexed data are then used to create orientation maps, which visually represent the crystallographic orientation of the grains within the material.

 

The results obtained from EBSD analysis are multifaceted and can provide comprehensive information about the microstructural characteristics of the material. Key outputs include orientation maps, grain boundary maps, phase maps, and pole figures. Orientation maps illustrate the spatial distribution of crystallographic orientations, revealing the size, shape, and orientation of individual grains. Grain boundary maps highlight the boundaries between grains, which are critical in understanding material properties such as mechanical strength and corrosion resistance. Phase maps identify different phases present in the sample, enabling phase distribution analysis. Pole figures offer a graphical representation of the crystallographic texture, indicating the preferred orientation of grains within the material.


EBSD phase maps

Phase maps are among the most important results from EBSD analysis, especially when characterizing materials with multiple phases. They prove crucial for understanding the material's properties by providing information about the phases present in the field of view and their distribution. Additionally, phase maps often indicate the proportion of each phase in the analyzed area. When phase characterization is conducted across thermal treatments or mechanical deformation, these maps can reveal information about phase transformations.

 

Grain boundaries are the interfaces where crystals of different orientations meet, significantly influencing material properties such as strength, toughness, corrosion resistance, and conductivity. Analyzing the distribution of these boundaries provides insights into the material's history, including deformation and recrystallization processes. Grain boundary distribution maps, generated from EBSD orientation data, visually represent different types of boundaries (low-angle and high-angle) using distinct colors or line types.

Phase map

EBSD grain size maps

Grain size map

Grain size maps offer a quantitative measure of the size and distribution of grains within a material. Grain size can be represented as the average diameter, area, or equivalent circular diameter of the grains. These maps are often color-coded based on grain size, allowing for a visual assessment of size variation and distribution.


EBSD inverse pole figures

Inverse pole figure (IPF) maps provide information on grain orientation. Colors indicate the crystal direction, with each map having a reference sample direction. The color assignment is based on the crystal orientation and the selected viewing direction. This information is crucial for understanding a material's preferred orientations or textures.

inverse pole figures

EBSD pole figures

Pole figures

Pole figures (PF) graphically represent the orientation of specific crystallographic planes or directions relative to the sample coordinate system using a stereographic projection. They are essential for understanding material texture, which describes the preferred orientation of grains in a sample. For polycrystalline materials with texture, crystal axes are not randomly distributed. To create a PF, a specific crystal direction (the pole) is chosen for each crystal relative to a set of directions in the material. Complete texture determination requires plotting two PFs for planes that are not parallel and do not have the same diffraction angle.


EBSD Euler maps

Euler maps provide detailed information about the crystallographic orientation of grains in a polycrystalline material, visualized using Euler angles. Euler angles define the orientation of a crystallographic plane or direction relative to a fixed coordinate system, describing the rotation needed to align the crystal’s coordinate system with the sample’s coordinate system. Each set of Euler angles corresponds to a unique color, creating a map where each grain or crystal orientation is represented by a specific color. The resulting Euler map visually represents the spatial distribution of crystallographic orientations across the sample.

Euler map

Kernel average misorientation maps

KAM map

Kernel average misorientation (KAM) maps quantify and visualize local variations in crystallographic orientation, making them useful for assessing the degree of plastic deformation and for identifying areas of local strain within a material. KAM measures the average misorientation between a central point and its neighboring points within the kernel (a small neighborhood around each measurement point on the sample), indicating local lattice distortions. KAM values are mapped using a color scale in which different colors represent varying degrees of misorientation.


EBSD image quality maps

Image quality (IQ) maps display the quality of the diffraction patterns obtained from the sample. Image quality refers to the clarity and sharpness of these patterns, with high-quality patterns having well-defined Kikuchi bands, while low-quality patterns may be blurred or indistinct. IQ is quantified using metrics based on the contrast and sharpness of Kikuchi bands. High IQ values generally correlate with reliable and accurate crystallographic orientation data, while low IQ values may highlight defects or variations in the sample's surface preparation.

Image quality map

Electron backscatter diffraction articles

EBSD Analysis of Metal and Alloy Microstructure

What is electron backscatter diffraction (EBSD)?

Combined EBSD and EDS Analysis

For Research Use Only. Not for use in diagnostic procedures.